[Determination of protocatechualdehyde in yu xue bi granula].
The content of Protocatechualdehyde in YuXueBi granula was determined by HPLC. The chromatographic column was packed with ODS-2 (particle size 5 microns). The mobile phase was MeOH-H2O-H3PO4(17:83:0.003) adjusted to pH 3 with N(C2H5)3. The detection wavelength was 280 nm. The velocity of flow was 1.0 ml/min. The average recovery rate was 96.14%, RSD was 1.16%. The method was simple and stable.
Dong
M
M
Shenyang Pharmaceutical University, Shenyang 11015.
Liu
X
X
Chen
F
F
Shi
M
M
D001547:Benzaldehydes / Q000032:analysis*; D002396:Catechols / Q000032:analysis*; D025924:Chromatography, Supercritical Fluid; D004338:Drug Combinations; D004365:Drugs, Chinese Herbal / Q000032:analysis*; D027561:Salvia miltiorrhiza / Q000737:chemistry
D001547:Benzaldehydes; D002396:Catechols; D004338:Drug Combinations; D004365:Drugs, Chinese Herbal; C005581:protocatechualdehyde