Preparation and characterisation of titania/hydroxyapatite composite coatings obtained by sol-gel process.
In the present work a titania network encapsulating a hydroxyapatite particulate phase is proposed as a bioceramic composite coating. The coating on a titanium substrate was produced starting from a sol containing a mixture of titania colloidal particles and hydroxyapatite submicron particles using the dip-coating technique. The microstructure, the morphology and the surface chemical composition of the coating were characterised using X-ray diffraction (XRD), scanning electron microscopy (SEM) and X-ray photoelectron spectroscopy (XPS), respectively. Adhesion tests were also performed. These analyses showed that the obtained coating was chemically clean, homogeneous, rough, porous, with a low thickness and well-defined phase composition as well as a good adhesion to the substrate.
Milella
E
E
Biomaterials Unit, Centro Nazionale per la Ricerca e Sviluppo Materiali, PASTIS-CNRSM, Brindisi, Italy. milella@cnrsm.it
Cosentino
F
F
Licciulli
A
A
Massaro
C
C
D001672:Biocompatible Materials; D017886:Durapatite; D004577:Electron Probe Microanalysis; D005782:Gels; D008855:Microscopy, Electron, Scanning; D014025:Titanium; D014961:X-Ray Diffraction
D001672:Biocompatible Materials; D005782:Gels; D017886:Durapatite; D014025:Titanium