title: The certification of SRM 1546--Meat Homogenate, a new reference material for nutrients in a high protein, high fat matrix.
abstract: In response to reference material needs expressed by the food industry and government regulators, the National Institute of Standards and Technology (NIST) has developed a new Standard Reference Material (SRM) consisting of a canned meat product with certified and reference values for a large number of constituents. SRM 1546 Meat Homogenate consists of a mixture of finely ground pork and chicken prepared and canned by a commercial process. NIST determined the concentration levels of cholesterol, sodium, calcium, iron, and seven fatty acids in this SRM using well defined methods and procedures. These analytes as well as 34 other constituents or properties were determined in an interlaboratory comparison exercise involving 21 laboratories, most of which are associated with the National Food Processors Association (NFPA) Food Industry Analytical Chemists Subcommittee (FIACS). From statistical analysis of the data, NIST assigned certified concentrations for the eleven analytes measured at NIST and reference concentrations for the proximates, six additional fatty acids, seven minerals, and seven water-soluble vitamins. Information values without uncertainties are provided for the concentrations of six additional constituents for which the uncertainties could not adequately be assessed. SRM 1546 will provide laboratories with a means to evaluate the accuracy of the methods they use to assign nutrient levels to processed meats and similar products.
authors.affiliation: Analytical Chemistry Division, United States Department of Commerce, Gaithersburg, MD 20899, USA. michael.welch@nist.gov
authors.forename: M J
authors.initials: MJ
authors.lastname: Welch
authors.forename: J C
authors.initials: JC
authors.lastname: Colbert
authors.forename: L M
authors.initials: LM
authors.lastname: Gill
authors.forename: C S
authors.initials: CS
authors.lastname: Phinney
authors.forename: K E
authors.initials: KE
authors.lastname: Sharpless
authors.forename: L T
authors.initials: LT
authors.lastname: Sniegoski
authors.forename: L J
authors.initials: LJ
authors.lastname: Wood
mesh_terms: D000818:Animals; D002645:Chickens; D002784:Cholesterol / Q000032:analysis; D004041:Dietary Fats / Q000032:analysis*; D004044:Dietary Proteins / Q000032:analysis*; D005504:Food Analysis; D005515:Food Labeling; D005519:Food Preservation / Q000592:standards*; D007753:Laboratories / Q000592:standards; D008460:Meat / Q000032:analysis* / Q000592:standards*; D015596:Nutrition Assessment; D009753:Nutritive Value; D011506:Proteins; D011786:Quality Control; D012015:Reference Standards; D012016:Reference Values; D013552:Swine
chemical_list: D004041:Dietary Fats; D004044:Dietary Proteins; D011506:Proteins; C429743:meat homogenate SRM 1546; D002784:Cholesterol