Determination of 241Am in sediments by isotope dilution high resolution inductively coupled plasma mass spectrometry (ID HR ICP-MS).
Trace levels (pg kg(-1)) of 241Am in sediments were determined by isotope dilution high resolution inductively coupled plasma mass spectrometry (ID HR ICP-MS) using a microconcentric nebulizer. 241Am was isolated from major elements like Ca and Fe by different selective precipitations. In further steps. Am was first separated from other transuranic elements and purified by anion exchange and extraction chromatography prior to the mass spectrometric measurements. The ID HR ICP-MS results are compared with isotope dilution alpha spectrometry.
Agarande
M
M
Environmental Radioactivity Measurement Laboratory, Institute for Nuclear Safety and Protection, Orsay, France. michele.agarande@ipsn.fr
Benzoubir
S
S
Bouisset
P
P
Calmet
D
D
D000465:Algorithms; D000512:Alpha Particles; D000576:Americium / Q000032:analysis* / Q000302:isolation & purification; D002852:Chromatography, Ion Exchange / Q000379:methods; D004307:Dose-Response Relationship, Radiation; D019015:Geologic Sediments / Q000737:chemistry*; D006801:Humans; D013058:Mass Spectrometry / Q000295:instrumentation / Q000379:methods; D011834:Radiation Monitoring / Q000295:instrumentation / Q000379:methods; D011865:Radioisotope Dilution Technique; D011868:Radioisotopes / Q000032:analysis*; D014501:Uranium / Q000032:analysis
D011868:Radioisotopes; D014501:Uranium; D000576:Americium