Cross-section preparation for transmission electron microscopy of phases and interfaces in C/BN heterostructures.
A technique is described for the preparation of transmission electron microscopy cross-sectional samples of pyrolytical carbon layers deposited on polycrystalline boron nitride substrates. To solve the problem of different abrasion rates of C and BN a filler material, Si wafers, has been bonded to both sides of the pre-thinned BN substrate. Correspondence between color and thickness of Si wafers facilitates controlled sample thickness reduction during dimpling. The samples prepared by this technique even without ion milling are thin enough for HRTEM studies.
Reznik
B
B
Laboratorium für Elektronenmikroskopie, Institut fur Chemische Technik der, Universität Karlsruhe, Kaiserstrasse 12, 76128, Karlsruhe, Germany. reznik@lem.uni-karlsruhe.de
Kalhöfer
S
S