Solid-state kinetics from time-resolved in situ XAFS investigations: reduction and oxidation of molybdenum oxides.
The reduction of MoO3 with hydrogen was studied by in situ X-ray absorption spectroscopy. The experiments performed focused on elucidating phase composition and evolution with time under isothermal reduction conditions. From temperature programmed experiments short-range structural details about the early stage of the reduction were obtained.
Ressler
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Fritz-Haber-Institut der Max-Planck-Gesellschaft, Department of Inorganic Chemistry, Berlin, Germany. Ressler@fhi-berlin.mpg.de
Jentoft
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Wienold
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Timpe
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