[Tocopherol Acetate Reference Standard (Control 001) of National Institute of Health Sciences].
The raw material of tocopherol acetate was examined for the preparation of the "Tocopherol Acetate Reference Standard (Control 001)". Analytical data obtained were: IR spectrum, same as that of the Tocopherol Acetate Reference Standard (Control 974); specific absorbance, E/cm% (284 nm) = 43.7; thin-layer chromatography, no impurities were detected until 50 micrograms of the loaded raw material; high-performance liquid chromatography (HPLC), total amount of impurities estimated to be less than 0.6%; assay by HPLC, 101.7%. Based on the above results, the raw material was authorized as the Japanese Pharmacopoeia Reference Standard (Control 001).
Iwata
M
M
Koide
T
T
Maekawa
K
K
Saito
H
H
Tanimoto
T
T
Okada
S
S
D002851:Chromatography, High Pressure Liquid; D002855:Chromatography, Thin Layer; D006077:Government Agencies; D007564:Japan; D010602:Pharmacopoeias as Topic; D012015:Reference Standards; D024505:Tocopherols; D024502:alpha-Tocopherol / Q000031:analogs & derivatives* / Q000032:analysis / Q000592:standards*
D024502:alpha-Tocopherol; D024505:Tocopherols