title: Convenient method for the preparation of 2'-deoxyribosylurea by thymidine oxidation and NMR study of both anomers.
abstract: The synthesis of 2'-deoxyribosylurea by thymidine oxidation with potassium permanganate followed by alkaline hydrolysis of intermediates is described. The anomeric configuration of the resulting products was studied by NMR spectroscopy.
authors.affiliation: Laboratoire de Chimie de Coordination du CNRS, Toulouse, France.
authors.forename: I
authors.initials: I
authors.lastname: Dubey
authors.forename: G
authors.initials: G
authors.lastname: Pratviel
authors.forename: A
authors.initials: A
authors.lastname: Robert
authors.forename: B
authors.initials: B
authors.lastname: Meunier
mesh_terms: D003855:Deoxyribose / Q000031:analogs & derivatives* / Q000138:chemical synthesis* / Q000737:chemistry; D007536:Isomerism; D009682:Magnetic Resonance Spectroscopy; D010084:Oxidation-Reduction; D013936:Thymidine / Q000737:chemistry*; D014508:Urea / Q000031:analogs & derivatives* / Q000138:chemical synthesis* / Q000737:chemistry
chemical_list: D003855:Deoxyribose; D014508:Urea; D013936:Thymidine