title: Resin-tooth adhesive interfaces after long-term function.
abstract: OBJECTIVE
  To characterize with scanning electron microscopy (SEM), the morphology of adhesive interfaces that had been functioning in an oral cavity for several years.
  
  
  METHODS
  Cavities were prepared in vivo in caries-affected primary molars under local anesthesia. After removal of the entire carious lesion, the cavity was restored with a dentin adhesive system (Scotchbond Multi-Purpose). After several yrs, as the successor permanent teeth erupted, the resin-filled teeth were extracted. Then, the extracted resin-restored primary molars were cross-sectioned perpendicular to the adhesive interface using a low speed diamond saw and then polished for SEM examination.
  
  
  RESULTS
  Morphological changes, such as digestion of the collagen fibrils and deterioration of the bonding resin and hybrid layer, were observed at the interface of the oral environment specimens. The results of this study demonstrated that degradation of resin-dentin bond structures appeared to occur in the human oral environment over time.
authors.affiliation: Department of Pediatric Dentistry, School of Dentistry, Hokkaido University, Sapporo, Japan. masanori-h@mue.biglobe.ne.jp
authors.forename: M
authors.initials: M
authors.lastname: Hashimoto
authors.forename: H
authors.initials: H
authors.lastname: Ohno
authors.forename: M
authors.initials: M
authors.lastname: Kaga
authors.forename: K
authors.initials: K
authors.lastname: Endo
authors.forename: H
authors.initials: H
authors.lastname: Sano
authors.forename: H
authors.initials: H
authors.lastname: Oguchi
mesh_terms: D002648:Child; D003188:Composite Resins; D001840:Dental Bonding; D003793:Dental Restoration, Permanent / Q000379:methods; D003804:Dentin / Q000648:ultrastructure; D003806:Dentin Permeability; D017220:Dentin-Bonding Agents; D024022:Fibrillar Collagens / Q000737:chemistry / Q000648:ultrastructure; D006801:Humans; D006868:Hydrolysis; D008855:Microscopy, Electron, Scanning; D008963:Molar; D019279:Resin Cements; D012822:Silicon Dioxide; D013499:Surface Properties; D013997:Time Factors; D014094:Tooth, Deciduous; D015040:Zirconium
chemical_list: D003188:Composite Resins; D017220:Dentin-Bonding Agents; D024022:Fibrillar Collagens; D019279:Resin Cements; C084018:Scotchbond Multi-Purpose; C083568:Z100 composite resin; D012822:Silicon Dioxide; D015040:Zirconium