title: Crystal structure of 4,6-O-ethylidene-N-(2-hydroxybenzylidene)-beta-D-glucopyranosylamine.
abstract: 4,6-O-Ethylidene-N-(2-hydroxybenzylidene)-beta-D-glucopyranosylamine was synthesized and characterized using analytical, spectral and single-crystal X-ray diffraction methods. The anomeric nature of the saccharide moiety was proposed based on 1H NMR studies and was confirmed by the crystal structure. The lattice structure of this compound was compared with that of its analogues.
authors.affiliation: Bioinorganic Laboratory, Department of Chemistry, Indian Institute of Technology Bombay, Powai, Mumbai 400 076, India.
authors.forename: Ajay K
authors.initials: AK
authors.lastname: Sah
authors.forename: Chebrolu P
authors.initials: CP
authors.lastname: Rao
authors.forename: Pauli K
authors.initials: PK
authors.lastname: Saarenketo
authors.forename: Kari
authors.initials: K
authors.lastname: Rissanen
mesh_terms: D003460:Crystallization; D005944:Glucosamine / Q000031:analogs & derivatives* / Q000138:chemical synthesis* / Q000737:chemistry*; D009682:Magnetic Resonance Spectroscopy / Q000379:methods; D015394:Molecular Structure; D014961:X-Ray Diffraction / Q000379:methods
chemical_list: C449504:4,6-O-Ethylidine-N-(2-hydroxybenzylidene)-glucopyranosylamine (H(3)L(1)); C075822:glucopyranosylamine; D005944:Glucosamine