Crystal structure of 4,6-O-ethylidene-N-(2-hydroxybenzylidene)-beta-D-glucopyranosylamine.
4,6-O-Ethylidene-N-(2-hydroxybenzylidene)-beta-D-glucopyranosylamine was synthesized and characterized using analytical, spectral and single-crystal X-ray diffraction methods. The anomeric nature of the saccharide moiety was proposed based on 1H NMR studies and was confirmed by the crystal structure. The lattice structure of this compound was compared with that of its analogues.
Sah
Ajay K
AK
Bioinorganic Laboratory, Department of Chemistry, Indian Institute of Technology Bombay, Powai, Mumbai 400 076, India.
Rao
Chebrolu P
CP
Saarenketo
Pauli K
PK
Rissanen
Kari
K
D003460:Crystallization; D005944:Glucosamine / Q000031:analogs & derivatives* / Q000138:chemical synthesis* / Q000737:chemistry*; D009682:Magnetic Resonance Spectroscopy / Q000379:methods; D015394:Molecular Structure; D014961:X-Ray Diffraction / Q000379:methods
C449504:4,6-O-Ethylidine-N-(2-hydroxybenzylidene)-glucopyranosylamine (H(3)L(1)); C075822:glucopyranosylamine; D005944:Glucosamine