Triterpenoid saponin from Primula elatior subsp. meyeri.
A new triterpenoid saponin, protoprimuloside B (2), has been isolated from the roots of Primula elatior subsp. meyeri and its structure deduced as 3beta-O-[[alpha-L-rhamnopyranosyl-(1-2)-beta-D-galactopyranosyl-(1-3)]-[beta-D-glucopyranosyl-(1-2)]-beta-D-glucopyranosyl]-protoprimuloside B by means of spectral data, especially NMR (400 MHz), including 1H, 13C, DEPT, COSY, HMBC, HMQC, NOESY techniques and (+)FAB-MS spectrum.
Yayli
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Karadeniz Technical University, Department of Chemistry, Trabzon, Turkey. yayli@ktu.edu.tr
D002850:Chromatography, Gel; D002855:Chromatography, Thin Layer; D008401:Gas Chromatography-Mass Spectrometry; D006851:Hydrochloric Acid / Q000737:chemistry; D009682:Magnetic Resonance Spectroscopy; D009904:Optical Rotation; D018517:Plant Roots / Q000737:chemistry; D029623:Primulaceae / Q000737:chemistry*; D012503:Saponins / Q000737:chemistry / Q000302:isolation & purification*; D017550:Spectroscopy, Fourier Transform Infrared; D014315:Triterpenes / Q000737:chemistry / Q000302:isolation & purification*
D012503:Saponins; D014315:Triterpenes; C451585:protoprimuloside B; D006851:Hydrochloric Acid