Synthesis and characterization of fluoro-substituted polyaniline.
Poly(2-fluoroaniline) was prepared by both chemical and electrochemical polymerization in acidic medium. Characterization of poly(2-fluoroaniline) was accomplished experimentally using ultraviolet-visible, Fourier transform infrared, differential scanning calorimetry, thermal gravimetric analysis, and X-ray diffraction techniques, respectively. Scanning electron microscopy studies revealed globular morphology of chemically synthesized poly(2-fluoroaniline). The cyclic voltammetric studies revealed diffusion-controlled phenomenon in electrochemically synthesized poly(2-fluoroaniline).
Sharma
A L
AL
Biomolecular Electronics and Conducting Polymer Research Group, National Physical Laboratory, New Delhi, India. alsharma@csnpl.ren.nic.in
Gerard
M
M
Singhal
R
R
Malhotra
B D
BD
Annapoorni
S
S
D000814:Aniline Compounds / Q000737:chemistry*; D004563:Electrochemistry; D008855:Microscopy, Electron, Scanning; D008956:Models, Chemical; D017550:Spectroscopy, Fourier Transform Infrared; D013696:Temperature; D014466:Ultraviolet Rays; D014961:X-Ray Diffraction
D000814:Aniline Compounds; C416807:polyaniline; C066212:2-fluoroaniline