[Study on the quality standards for xianghe suppository].
The quality standards for Xianghe suppository were studied. The TLC methods for identification of Rhizoma Coptidis, Radix Sophorae Flavescentis and Flos Caryophylli were established. A simple high performance liquid chromatographic method was established for determination of berberine and palmatine. The mobile phase was acetonitrile-water(1:1, containing KH2PO4 3.4 g, CH3(CH2)11 SO4Na 1.7 g per 1000 ml). UV detecting wavelength was 345 nm. This method is suitable for the quality control of Xianghe suppository.
Deng
Y
Y
Guangdong Provincial Hospital of TCM, Guangzhou 510120.
Yang
L
L
Qiu
X
X
Dong
Y
Y
D001599:Berberine / Q000032:analysis; D001600:Berberine Alkaloids / Q000032:analysis; D002851:Chromatography, High Pressure Liquid; D002855:Chromatography, Thin Layer; D004365:Drugs, Chinese Herbal / Q000032:analysis / Q000592:standards*; D011786:Quality Control; D013488:Suppositories
D001600:Berberine Alkaloids; D004365:Drugs, Chinese Herbal; D013488:Suppositories; D001599:Berberine; C005413:palmatine