title: The extent to which resin can infiltrate dentin by acetone-based adhesives.
abstract: The combined methodologies of fractography and laser-Raman spectroscopic analysis were used for evaluation of the resin-dentin bonds made with wet and dry bonding. Resin-dentin-bonded beams were produced by means of 2 acetone-based adhesives (One-Step and Prime & Bond NT). The micro-tensile bond test was conducted, and the fractured surfaces of all specimens were examined by SEM and an image analyzer. The amount of resin infiltration within the hybrid layer was quantified by means of a laser-Raman spectroscope. In Raman analysis, the amount of resin impregnation within the hybrid layer of the dry bonding was found to be significantly lower (approximately 50%) than that in the wet one. Under fractographic analysis, a correlation was found between the bond strength and the failure mode. Based on those findings, it was suggested that the integrity between the bonding resin and the top of the hybrid layer played a major role in bond strength.
authors.affiliation: Department of Operative Dentistry and Endodontics, Iwate Medical University, School of Dentistry, Morioka, Japan. masanori-h@mue.biglobe.ne.jp
authors.forename: M
authors.initials: M
authors.lastname: Hashimoto
authors.forename: H
authors.initials: H
authors.lastname: Ohno
authors.forename: M
authors.initials: M
authors.lastname: Kaga
authors.forename: H
authors.initials: H
authors.lastname: Sano
authors.forename: K
authors.initials: K
authors.lastname: Endo
authors.forename: H
authors.initials: H
authors.lastname: Oguchi
mesh_terms: D000096:Acetone / Q000737:chemistry; D000704:Analysis of Variance; D001641:Bicuspid; D017438:Bisphenol A-Glycidyl Methacrylate; D020770:Compomers; D003188:Composite Resins; D001840:Dental Bonding; D003806:Dentin Permeability; D017220:Dentin-Bonding Agents / Q000737:chemistry*; D003890:Desiccation; D006801:Humans; D008422:Materials Testing; D008689:Methacrylates / Q000737:chemistry; D008855:Microscopy, Electron, Scanning; D011109:Polymethacrylic Acids / Q000737:chemistry; D012044:Regression Analysis; D019279:Resin Cements / Q000737:chemistry*; D012821:Silanes; D017640:Silicates; D012822:Silicon Dioxide; D013059:Spectrum Analysis, Raman; D013499:Surface Properties; D013718:Tensile Strength
chemical_list: C098721:Aelitefil; C103506:Bis-GMA, BPDM, HEMA dental-bonding resin; D020770:Compomers; D003188:Composite Resins; D017220:Dentin-Bonding Agents; C088486:Dyract; D008689:Methacrylates; D011109:Polymethacrylic Acids; C425843:Prime and Bond NT; D019279:Resin Cements; D012821:Silanes; D017640:Silicates; D000096:Acetone; D017438:Bisphenol A-Glycidyl Methacrylate; D012822:Silicon Dioxide