Two-dimensional and variable temperature 31P solid-state NMR studies of single crystals containing symmetrical/unsymmetrical bis[6-O,6-O'-(1,2:3,4-diisopropylidene-alpha-D- galactopyranosyl)thiophosphoryl] dichalcogenides.
The organisation and phase transition of single crystals containing three isostructural bis[6-O,6-O'-(1,2:3,4-diisopropylidene-alpha- D-galactopyranosyl)thiophosphoryl] dichalcogenide derivatives: disulfide 1, diselenide 2 and mixed seleno-sulfide 3, was deduced upon 1D, 2D and variable temperature 31P NMR experiments.
Potrzebowski
M J
MJ
Department of Structural Studies, Centre of Molecular and Macromolecular Studies, Polish Academy of Sciences, Sienkiewicza 112, PL-90-363 Łódź, Poland. marekpot@bilbo.cbmm.lodz.pl
Helinski
J
J
Ciesielski
W
W