Development of an HPLC-NMR method for the determination of PAHs in soil samples - a comparison with conventional methods.
A hyphenated HPLC-(1)H NMR method for the identification and quantification of PAHs in soil samples has been developed and applied to a PAH reference sample provided by the Federal Institute for Materials Research and Testing (BAM, Berlin, Germany). The results were compared with those obtained by HPLC-DAD, HPLC-F, and GC-MS analyses of the same sample.
Weisshoff
Hardy
H
Humboldt University of Berlin, Institute of Chemistry, Germany.
Preiss
Alfred
A
Nehls
Irene
I
Win
Tin
T
Mügge
Clemens
C
D002851:Chromatography, High Pressure Liquid / Q000379:methods*; D008401:Gas Chromatography-Mass Spectrometry; D009682:Magnetic Resonance Spectroscopy / Q000379:methods*; D011083:Polycyclic Compounds / Q000032:analysis*; D012015:Reference Standards; D012680:Sensitivity and Specificity; D012989:Soil Pollutants / Q000032:analysis*
D011083:Polycyclic Compounds; D012989:Soil Pollutants