Structural analysis of partially acetylated glycosides by refocused-decoupled insensitive nuclei enhanced by polarization transfer (INEPT) experiments: a qualitative and quantitative method.
The application of the refocused-decoupled INEPT pulse sequence in 13C-NMR spectroscopy allows, in conjonction with computer simulations, a straightforward editing of the spectra of a raw mixture of glycosidic compounds.
Institut du Pin (EA 494), Laboratoire de Chimie des Substances Végétales, Université Bordeaux I, Talence, France.
Laurent
L
Pouységu
Bernard
B
De Jéso
Jean-Claude
JC
Lartigue
Michel
M
Pétraud
Max
M
Ratier
D000107:Acetylation; D006027:Glycosides / Q000032:analysis* / Q000737:chemistry*; D015394:Molecular Structure; D019906:Nuclear Magnetic Resonance, Biomolecular / Q000379:methods
D006027:Glycosides