[Determination of columbianetin, columbianetin acetate and osthol in Angelica pubescens Maxim. f. biserrata Shan et Yuan by HPLC].
OBJECTIVE
To develop a method for the determination of columbianetin, columbianetin acetate and osthol in Angelica pubescens f. biserrata


METHODS
HPLC method, ODS column (6.0 mm x 150 mm) with a mobile phase of methanol-acetonitrile-0.025 mol.L-1 phosphoric acid (32:20:48), and wave length detection at 320 nm.


CONCLUSIONS
The method can be used for the quality control of raw medicinal materials.
Department of Traditional Chinese Pharmacy, Liaoning College of Traditional Chinese Medicine, Shenyang 110032.
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Cai
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Sha
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Yang
D029969:Angelica / Q000737:chemistry*; D002851:Chromatography, High Pressure Liquid; D003374:Coumarins / Q000737:chemistry / Q000302:isolation & purification*; D004365:Drugs, Chinese Herbal / Q000032:analysis*; D011564:Furocoumarins / Q000737:chemistry / Q000302:isolation & purification*; D018517:Plant Roots / Q000737:chemistry; D010946:Plants, Medicinal / Q000737:chemistry*
D003374:Coumarins; D004365:Drugs, Chinese Herbal; D011564:Furocoumarins; C046733:columbianetin; C076302:columbianetin acetate; C046627:osthol