Trapping of benzene oxide-oxepin and methyl-substituted derivatives with 4-phenyl- and 4-pentafluorophenyl-1,2,4-triazoline-3,5-dione.
4-Phenyl-1,2,4-triazoline-3,5-dione and its pentafluoro analogue are efficient reagents for trapping arene oxides, e.g. benzene oxide-oxepin, affording crystalline adducts that can be quantitatively analysed by HPLC and MS techniques.
Henderson
Alistair P
AP
Department of Chemistry, Bedson Building, University of Newcastle upon Tyne, Newcastle upon Tyne, UK NEI 7RU.
Mutlu
Esra
E
Leclercq
Amélie
A
Bleasdale
Christine
C
Clegg
William
W
Henderson
Richard A
RA
Golding
Bernard T
BT