title: Gas chromatography for in situ analysis of a cometary nucleus. IV. Study of capillary column robustness for space application.
abstract: As part of the development of the European Space Agency Rosetta space mission to investigate a cometary nucleus, the selection of columns dedicated to the gas chromatographic subsystem of the Cometary Sampling and Composition (COSAC) experiment was achieved. Once the space probe launched, these columns will be exposed to the harsh environmental constraints of space missions: vibrations, radiation (by photons or energetic particles), space vacuum, and large temperature range. In order to test the resistance of the flight columns and their stationary phases, the columns were exposed to these rough conditions reproduced in the laboratory. The comparison of the analytical performances of the columns, evaluated prior and after the environmental tests, demonstrated that all the columns withstand space constraints, and that their analytical properties were preserved. Therefore, all the selected capillary columns, even having porous layer or chiral stationary phases, were qualified for space exploration.
authors.affiliation: Laboratoire Interuniversitaire des Systèmes Atmosphériques, UMR 7583, CNRS, Université Paris 7 and Paris 12, C.M.C., 61 Avenue du Général de Gaulle, 94010 Créteil, France. cyril.szopa@aerov.jussieu.fr
authors.forename: C
authors.initials: C
authors.lastname: Szopa
authors.forename: U J
authors.initials: UJ
authors.lastname: Meierhenrich
authors.forename: D
authors.initials: D
authors.lastname: Coscia
authors.forename: L
authors.initials: L
authors.lastname: Janin
authors.forename: F
authors.initials: F
authors.lastname: Goesmann
authors.forename: R
authors.initials: R
authors.lastname: Sternberg
authors.forename: J F
authors.initials: JF
authors.lastname: Brun
authors.forename: G
authors.initials: G
authors.lastname: Israel
authors.forename: M
authors.initials: M
authors.lastname: Cabane
authors.forename: R
authors.initials: R
authors.lastname: Roll
authors.forename: F
authors.initials: F
authors.lastname: Raulin
authors.forename: W
authors.initials: W
authors.lastname: Thiemann
authors.forename: C
authors.initials: C
authors.lastname: Vidal-Madjar
authors.forename: H
authors.initials: H
authors.lastname: Rosenbauer
mesh_terms: D002849:Chromatography, Gas / Q000295:instrumentation*; D019110:Meteoroids; D013026:Space Flight