Screening method for polycyclic aromatic hydrocarbons in soil using hollow fiber membrane solvent microextraction.
A fast, inexpensive screening method for polycyclic aromatic hydrocarbons in soil has been developed. Using hollow fiber membrane solvent microextraction, 8 microl of octane extraction solvent was placed inside a porous, polypropylene fiber. Following an 8 min analyte preconcentration step, 4 microl of extract was injected into a gas chromatograph. Separation was achieved in less than 10 min with a detection limit of 0.13 mg/kg for 2-methylnaphthalene. Results of both spiked and real soil samples are presented.
King
Stephanie
S
Department of Chemistry and Biochemistry, Ohio University, Athens, OH 45701-2979, USA. sk352800@ohio.edu
Meyer
Jill S
JS
Andrews
Anthony R J
AR
D002138:Calibration; D008567:Membranes, Artificial; D011083:Polycyclic Compounds / Q000032:analysis*; D012680:Sensitivity and Specificity; D012989:Soil Pollutants / Q000032:analysis*; D012997:Solvents / Q000737:chemistry*
D008567:Membranes, Artificial; D011083:Polycyclic Compounds; D012989:Soil Pollutants; D012997:Solvents