[Simultaneous determination of fluoroacetamide and tetramethylendisulfotetramin with gas chromatography-mass spectrography].
Simultaneous determination of fluoroacetamide and tetramethylendisulfotetramin with gas chromatography-mass spectrography was established. The condition of separation, ways of extraction, the qualitative and quantitative determination of two compounds were discussed. The linear ranges of fluoroacetamide and tetramethylendisulfotetramin were 5-40 micrograms/ml and 0.5-20.0 micrograms/ml, respectively. The recoveries of these two compounds in different sample were 52.25%-94.30% and 61.85%-92.50%, respectively. The method was fast, sensitive and accurate.
Ma
Y
Y
Feng
F
F
Chen
B
B
D001952:Bridged-Ring Compounds / Q000032:analysis*; D005463:Fluoroacetates / Q000032:analysis*; D008401:Gas Chromatography-Mass Spectrometry
D001952:Bridged-Ring Compounds; D005463:Fluoroacetates; C007741:fluoroacetamide; C010349:tetramethylenedisulfotetramine