title: [Application of wide-bore capillary gas chromatography in the synthesis of special esters of methacrylic acid].
abstract: A simple, rapid and accurate method for separating and analysing components in the synthesis of special esters of methacrylic acid by gas chromatography is reported. An SE-54 wide-bore capillary column of 50 m x 0.53 mm i.d. x 0.6 microns was used. The esters include dimethylaminoethyl methacrylate(DMAM), n-butyl methacrylate(BMA) and ethylene glycol dimethacrylate(EGDMA). Crude materials such as methyl methacrylate(MMA) and N, N-dimethyl ethanol amine (DMEA) were also analysed. The recoveries were 99.71%-102.89%, and the RSDs of the main components were below 0.1%. The method can be used to control the production of the esters.
authors.affiliation: Research Institute of Qilu Petrochemical Co., Zibo 255400, China.
authors.forename: F F
authors.initials: FF
authors.lastname: Liu
authors.forename: J
authors.initials: J
authors.lastname: Sun
authors.forename: F S
authors.initials: FS
authors.lastname: Liu
authors.forename: H C
authors.initials: HC
authors.lastname: Liang