[Simultaneous determination of fluoroacetamide and tetramine by gas chromatography].
A simple and fast gas chromatographic method was used for the simultaneous determination of fluoroacetamide and tetramine. The samples were extracted with acetone and the extracts were analyzed by gas chromatography. A megabore capillary column coated with FFAP and a nitrogen-phosphorous detector were used to obtain satisfactory selectivity and sensitivity. The detection limits and average recoveries were 5 ng and 69.1% for fluoroacetamide and 1 ng and 89.8% for tetramine.
Wu
Qing
Q
Center of Analysis and Test, Guizhou Normal University, Guiyang 550001, China.
Zhang
Ming-shi
MS
Lan
Zhao-rong
ZR
D001952:Bridged-Ring Compounds / Q000032:analysis*; D002849:Chromatography, Gas / Q000295:instrumentation* / Q000379:methods; D005463:Fluoroacetates / Q000032:analysis*; D012378:Rodenticides / Q000032:analysis*
D001952:Bridged-Ring Compounds; D005463:Fluoroacetates; D012378:Rodenticides; C007741:fluoroacetamide; C010349:tetramethylenedisulfotetramine