Fractionation of starch hydrolysates into dextrins with narrow molecular mass distribution and their detection by high-performance anion-exchange chromatography with pulsed amperometric detection.
Low levels of high-molecular-mass dextrins in starch hydrolysates can be detected by high-performance anion-exchange chromatography with pulsed amperometric detection in spite of their low responses by dialysis of the starch hydrolysate and fractionation of the resulting adialysate with ethanol (final concentration 30-80% at 6 degrees C). In doing so, dextrin fractions with a relatively narrow molecular mass distribution were obtained.
Gelders
Greta G
GG
Laboratory of Food Chemistry, Katholieke Universiteit Leuven, Kasteelpark Arenberg 20, B-3001 Leuven, Belgium. greet.gelders@agr.kuleuven.ac.be
Bijnens
Lieve
L
Loosveld
Anne-Marie
AM
Vidts
An
A
Delcour
Jan A
JA
D000837:Anion Exchange Resins; D002851:Chromatography, High Pressure Liquid / Q000379:methods*; D002852:Chromatography, Ion Exchange / Q000379:methods*; D003912:Dextrins / Q000737:chemistry / Q000302:isolation & purification*; D004563:Electrochemistry / Q000379:methods*; D006868:Hydrolysis; D008970:Molecular Weight; D013213:Starch / Q000737:chemistry*
D000837:Anion Exchange Resins; D003912:Dextrins; D013213:Starch