Determination of residual pesticides in olive oil by GC-MS and HPLC-MS after extraction by size-exclusion chromatography.
This work describes the development of a method for analyzing pesticide residues in olive oil by GC-MS and HPLC-MS. Pesticides were separated from the oily matrix by size-exclusion chromatography. After extraction, 20 pesticides were separated and analyzed by GC-MS and 11 others HPLC-MS in electrospray mode. The development of this method enabled us to identify and quantify the pesticides of interest.
Barrek
Sami
S
Service Central d'Analyse, USR 059, CNRS, BP 22, 69390 Vernaison, France.
Paisse
Olivier
O
Grenier-Loustalot
Marie-Florence
MF
D002850:Chromatography, Gel / Q000379:methods*; D002851:Chromatography, High Pressure Liquid / Q000379:methods*; D008401:Gas Chromatography-Mass Spectrometry / Q000379:methods*; D000069463:Olive Oil; D010573:Pesticide Residues / Q000032:analysis*; D010938:Plant Oils / Q000737:chemistry*; D021241:Spectrometry, Mass, Electrospray Ionization / Q000379:methods*
D000069463:Olive Oil; D010573:Pesticide Residues; D010938:Plant Oils