[Direct determination of Cu and Pb in edible L-lysine by graphite furnace atomic absorption spectrometry].
The determination of Cu and Pb in edible L-lysine by rapid graphite furnace atomic absorption spectrometry (GFAAS) is described in this paper. The sample is dissolved with thin acid and mensurated directly by GFAAS. It does not need dry ashing and wet digesting and without chemical matrix modifier. The Graphite Furnace's function of pre-treatment is fully used. Results can be obtained as soon as possible and avoid unnecessary contamination and loss of samples. The method is simple, rapid, practical and have good precision and accurate. Under the optimum conditions the result indicates that the relative standard deviation of Cu and Pb is 4.8% and 5.3% respectively, the recovery rate is 100%-110% and 102%-105% separately.
Shan
Fang
F
Institute of Agricultural Products Comprehensive Utilization, Shanxi Academy of Agriculture Sciences, Taiyuan 030031, China.
Bian
Jun-sheng
JS
D003300:Copper / Q000032:analysis*; D005527:Food, Fortified / Q000032:analysis*; D006108:Graphite; D007854:Lead / Q000032:analysis*; D008239:Lysine / Q000737:chemistry*; D013054:Spectrophotometry, Atomic / Q000379:methods
D007854:Lead; D006108:Graphite; D003300:Copper; D008239:Lysine