title: [Determination of lead and arsenic in copper aspirinate by graphite furnace atomic absorption spectrometry].
abstract: A graphite furnace atomic absorption spectrometric method has been established to determine trace lead and arsenic in copper aspirinate, a new anti-inflammatory and anti-thrombotic agent. The sample is pretreated by ashing at 530 degrees C in the presence of Ni (NO3)2, followed by dissolution with HNO3. The method is simple and has a low detection limit. The relative standard deviation is 11%-15%, the recovery is 92%-112% for lead and 86%-119% for arsenic.
authors.affiliation: Kunming Instiute of Precious Metals, 650221 Kunming.
authors.forename: H
authors.initials: H
authors.lastname: Qiu
authors.forename: J
authors.initials: J
authors.lastname: Liu
mesh_terms: D000894:Anti-Inflammatory Agents, Non-Steroidal / Q000737:chemistry*; D001151:Arsenic / Q000032:analysis*; D001241:Aspirin / Q000031:analogs & derivatives* / Q000737:chemistry*; D007854:Lead / Q000032:analysis*; D013054:Spectrophotometry, Atomic / Q000379:methods
chemical_list: D000894:Anti-Inflammatory Agents, Non-Steroidal; C027058:tetrakis-mu-acetylsalicylato-dicopper(II); D007854:Lead; D001151:Arsenic; D001241:Aspirin