[Determination of Hg and As in crude antimony trioxide by microwave process system and ICP-AES].
An ICP-AES method was established for the simultaneous determination of Hg and As in crude antimony trioxide. The samples with different grades were digested in hydrochloric acid-tartraic acid-potassium chloride using microwave process system. The method is applied to analyze crude antimony trioxide with RSD% of 0.87%-3.2% for Hg, 1.3%-2.9% for As, and recovery of 90%-107%
Zhong
Y
Y
Shenzhen Entry-Exit Inspection and Quarntine Bureau, 518045 Shenzhen.
He
H
H
Zhang
Q
Q
D000965:Antimony / Q000737:chemistry*; D001149:Arsenates / Q000032:analysis*; D008628:Mercury / Q000032:analysis*; D008872:Microwaves; D013054:Spectrophotometry, Atomic / Q000379:methods
D001149:Arsenates; D000965:Antimony; D008628:Mercury; C037554:antimony trioxide