Comparison of yield, composition, and antioxidant activity of turmeric (Curcuma longa L.) extracts obtained using various techniques.
Turmeric extracts were obtained from two lots of raw material (M and S) using various techniques: hydrodistillation, low pressure solvent extraction, Soxhlet, and supercritical extraction using carbon dioxide and cosolvents. The solvents and cosolvents tested were ethanol, isopropyl alcohol, and their mixture in equal proportions. The composition of the extracts was determined by gas chromatography-flame ionization detection (GC-FID) and UV. The largest yield (27%, weight) was obtained in the Soxhlet extraction (turmeric (S), ethanol = 1:100); the lowest yield was detected in the hydrodistillation process (2.1%). For the supercritical extraction, the best cosolvent was a mixture of ethanol and isopropyl alcohol. Sixty percent of the light fraction of the extracts consisted of ar-turmerone, (Z)-gamma-atlantone, and (E)-gamma-atlantone, except for the Soxhlet extracts (1:100, ethanol), for which only ar-turmeronol and (Z)-alpha-atlantone were detected. The maximum amount of curcuminoids (8.43%) was obtained using Soxhlet extraction (ethanol/isopropyl alcohol). The Soxhlet and low pressure extract exhibited the strongest antioxidant activities.
Braga
Mara E M
ME
LASEFI, DEA/FEA (College of Food Engineering), UNICAMP (State University of Campinas), Caixa Postal 6121, 13083-970 Campinas, SP, Brazil.
Leal
Patrícia F
PF
Carvalho
João E
JE
Meireles
M Angela A
MA
D000975:Antioxidants / Q000032:analysis* / Q000737:chemistry; D002849:Chromatography, Gas; D025924:Chromatography, Supercritical Fluid; D030024:Curcuma / Q000254:growth & development; D003474:Curcumin / Q000032:analysis; D005511:Food Handling / Q000379:methods*; D007659:Ketones / Q000032:analysis; D010936:Plant Extracts / Q000737:chemistry*; D012717:Sesquiterpenes; D012997:Solvents; D014050:Toluene / Q000031:analogs & derivatives* / Q000032:analysis
D000975:Antioxidants; D007659:Ketones; D010936:Plant Extracts; D012717:Sesquiterpenes; D012997:Solvents; C078098:ar-turmerone; D014050:Toluene; C012596:turmeric extract; D003474:Curcumin