Determination of volatile aliphatic amines in air by solid-phase microextraction coupled with gas chromatography with flame ionization detection.
Practical aspects of the application of solid-phase microextraction (SPME) to the determination of volatile aliphatic amines in air are described. Analytes included methylamine (MA), ethylamine (EA), dimethylamine (DMA), diethylamine (DEA), trimethylamine (TMA) and triethylamine (TEA). New SPME stationary phases were examined. The effects of relative humidity and temperature on analytes uptake were taken into account in analysis. Gas chromatography (GC) with flame ionization detector (FID) was used for the final analysis.
Namieśnik
Jacek
J
Department of Analytical Chemistry, Chemical Faculty, Gdańsk University of Technology, 11/12 G. Narutowicza Street, 80-952 Gdańsk, Poland. chemanal@pg.gda.pl
Jastrzebska
Anna
A
Zygmunt
Bogdan
B
D000388:Air / Q000032:analysis*; D000588:Amines / Q000032:analysis*; D002138:Calibration; D002849:Chromatography, Gas / Q000379:methods*; D013696:Temperature; D014835:Volatilization
D000588:Amines