An application of the XiX decoupling for solid state 13C NMR with mobile samples.
It is very important to obtain higher resolution solid state NMR spectra not only for crystal samples but also for mobile solid samples. We demonstrate that a robust proton decoupling technique, XiX (X inverse-X) decoupling, is very effective in high resolution solid state NMR measurement for mobile samples compared with the usual continuous wave proton decoupling.
Ashida
Jun
J
Varian Technologies Japan Ltd., 4-16-36 Shibaura, Minato, 108-0023, Tokyo, Japan. jun.ashida@varianinc.com
Asakura
Tetsuo
T
D000218:Adamantane / Q000737:chemistry*; D002247:Carbon Isotopes; D005240:Feasibility Studies; D045782:Hemiterpenes; D007840:Latex; D009682:Magnetic Resonance Spectroscopy / Q000379:methods*; D009038:Motion; D011095:Polyethylenes / Q000737:chemistry*; D011522:Protons; D013113:Spin Labels
D002247:Carbon Isotopes; D045782:Hemiterpenes; D007840:Latex; D011095:Polyethylenes; D011522:Protons; D013113:Spin Labels; C455100:1,4-polyisoprene; D000218:Adamantane