title: A versatile synthesis of new pyrimidinyl nitronyl nitroxides.
abstract: Pyrimidinyl nitronyl nitroxides where the bis-N-oxy fragment is included in a six-membered ring were prepared from diacetonamine by a sequence of reactions including a Grignard reaction, a Ritter reaction and oxidation of the intermediate pyrimidine; the properties of the 2-phenyl-substituted representative are fully described.
authors.affiliation: Département de Recherche Fondamentale sur la Matiére Condensée, Service de Chimie Inorganique et Biologique, (UMR CNRS 5046), 17 Rue des Martyrs F38054, Grenoble Cedex 09, France.
authors.forename: P
authors.initials: P
authors.lastname: Brough
authors.forename: R
authors.initials: R
authors.lastname: Chiarelli
authors.forename: J
authors.initials: J
authors.lastname: Pécaut
authors.forename: A
authors.initials: A
authors.lastname: Rassat
authors.forename: P
authors.initials: P
authors.lastname: Rey