Field gas chromatography-mass spectrometry for fast analysis.
The objective of this presentation is to demonstrate the original device and procedure for fast gas chromatography-mass spectrometry (GC-MS) analysis of gaseous and liquid samples and to discuss its features and capabilities. The concept was developed in order to expand the range of compounds suitable for GC separation and to reduce the time of analysis. Field GC-MS, consisting of original "concentrator-thermodesorber" (CTD) unit, multiple module GC system and compact magnetic mass spectrometer with powerful two-stage vacuum system and multicollector ion detector, is represented. The whole weight of the device is 90 kg. Power consumption is 250 W. The device and analytical procedures allow high speed screening of toxic substances in air and extracts within 100 s per sample. The examples of applications are described, including fast screening of tributyl phosphate (TBP) in air at low ppt level at the rate 1 sample/min.
Makas
Alexei L
AL
Design Technological Institute of Instrument Engineering for Geophysics and Ecology, Siberian Branch of the Russian Academia of Sciences, 3/6 Academician Koptyug Avenue, Novosibirsk 630090, Russia. glue@uiggm.nsc.ru
Troshkov
Mikhail L
ML
D000336:Aerosols / Q000032:analysis; D000388:Air / Q000032:analysis; D002619:Chemical Warfare Agents / Q000032:analysis; D008401:Gas Chromatography-Mass Spectrometry / Q000295:instrumentation*; D005740:Gases / Q000032:analysis; D013058:Mass Spectrometry / Q000295:instrumentation; D010755:Organophosphates / Q000032:analysis; D013997:Time Factors
D000336:Aerosols; D002619:Chemical Warfare Agents; D005740:Gases; D010755:Organophosphates; C009524:tributyl phosphate