title: [Estrone Reference Standard (Control 021) of National Institute of Health Sciences].
abstract: The raw material of estrone acetate was examined for the preparation of the "Estrone Reference Standard (Control 021)", The analytical data obtained were: UV spectrum, lambda max of 281 nm and specific absorbance in ethanol at 281 nm = 76.1; Melting point, 261.6 degrees C; IR spectrum, exhibited the specific absorptions at 3345, 2867, 1720, 1499 and 1055 cm-1; thin-layer chromatography, 2 impurities were detected at 100 and 200 micrograms; high-performance liquid chromatography, total amount of impurities estimated to be less than 0.3%. Based on the above results, the raw material was authorized as Estrone Reference Standard (Control 021) of the National Institute of Health Sciences.
authors.forename: Miho
authors.initials: M
authors.lastname: Murakami
authors.forename: Yukiko
authors.initials: Y
authors.lastname: Morita
authors.forename: Tatsuo
authors.initials: T
authors.lastname: Koide
authors.forename: Hiroyuki
authors.initials: H
authors.lastname: Saito
authors.forename: Tsuyoshi
authors.initials: T
authors.lastname: Tanimoto
mesh_terms: D002851:Chromatography, High Pressure Liquid; D004970:Estrone / Q000032:analysis / Q000592:standards*; D006077:Government Agencies; D007564:Japan; D010602:Pharmacopoeias as Topic / Q000592:standards; D012015:Reference Standards
chemical_list: D004970:Estrone