Electron holography on remanent magnetization distribution of melt-spun Nd-Fe-B magnets.
Microstructures and magnetic domain structures of melt-spun Nd-Fe-B permanent magnets were investigated in detail by analytical electron microscopy and electron holography. While the crystal orientation of matrix Nd2Fe14B grains was analyzed by nanobeam electron diffraction, precipitates of a few tens of nanometers at grain boundaries were identified to be alpha-Fe by energy-dispersive X-ray spectroscopy. The detailed magnetization distribution in Nd2Fe14B grains and at their boundaries was visualized by electron holography. Ex situ experimentation with an electromagnet revealed that the domain walls in the demagnetized state and remanent states were pinned at grain boundaries, and Fe precipitates at the grain boundary were situated at the center of the closure domain.
Park
Young-Gil
YG
Shindo
Daisuke
D
D001895:Boron / Q000737:chemistry*; D006696:Holography; D007501:Iron / Q000737:chemistry*; D008280:Magnetics; D008854:Microscopy, Electron; D009354:Neodymium / Q000737:chemistry*; D013052:Spectrometry, X-Ray Emission
D009354:Neodymium; D007501:Iron; D001895:Boron