title: Analysis of tensile bond strengths using Weibull statistics.
abstract: Tensile strength tests of restorative resins bonded to dentin, and the resultant strengths of interfaces between the two, exhibit wide variability. Many variables can affect test results, including specimen preparation and storage, test rig design and experimental technique. However, the more fundamental source of variability, that associated with the brittle nature of the materials, has received little attention. This paper analyzes results from micro-tensile tests on unfilled resins and adhesive bonds between restorative resin composite and dentin in terms of reliability using the Weibull probability of failure method. Results for the tensile strengths of Scotchbond Multipurpose Adhesive (3M) and Clearfil LB Bond (Kuraray) bonding resins showed Weibull moduli (m) of 6.17 (95% confidence interval, 5.25-7.19) and 5.01 (95% confidence interval, 4.23-5.8). Analysis of results for micro-tensile tests on bond strengths to dentin gave moduli between 1.81 (Clearfil Liner Bond 2V) and 4.99 (Gluma One Bond, Kulzer). Material systems with m in this range do not have a well-defined strength. The Weibull approach also enables the size dependence of the strength to be estimated. An example where the bonding area was changed from 3.1 to 1.1 mm diameter is shown. Weibull analysis provides a method for determining the reliability of strength measurements in the analysis of data from bond strength and tensile tests on dental restorative materials.
authors.affiliation: School of Dental Science, The University of Melbourne, Victoria 3010, Melbourne, Australia. mfburrow@unimelb.edu.au
authors.forename: Michael F
authors.initials: MF
authors.lastname: Burrow
authors.forename: David
authors.initials: D
authors.lastname: Thomas
authors.forename: Mike V
authors.initials: MV
authors.lastname: Swain
authors.forename: Martin J
authors.initials: MJ
authors.lastname: Tyas
mesh_terms: D000134:Acid Etching, Dental; D000269:Adhesives / Q000737:chemistry*; D003188:Composite Resins / Q000737:chemistry*; D001840:Dental Bonding; D003738:Dental Cements; D003804:Dentin / Q000737:chemistry; D017220:Dentin-Bonding Agents / Q000737:chemistry*; D008422:Materials Testing; D015233:Models, Statistical; D019279:Resin Cements / Q000737:chemistry*; D013048:Specimen Handling; D013718:Tensile Strength
chemical_list: D000269:Adhesives; D003188:Composite Resins; D003738:Dental Cements; D017220:Dentin-Bonding Agents; D019279:Resin Cements; C041330:Scotchbond