title: Complete assignments of 1H and 13C NMR data for 10 phenylethanoid glycosides.
abstract: Ten phenylethanoid glycosides, including two new ones, isolated from the aerial parts of the mangrove plant Acanthus ilicifolius were identified. The first complete assignments of the 1H and 13C NMR chemical shifts for these glycosides were achieved by means of 2D NMR techniques, including 1H-1H COSY, TOCSY, HSQC and HMBC spectra.
authors.affiliation: Guangdong Key Laboratory of Marine Materia Medica, South China Sea Institute of Oceanology, Chinese Academy of Sciences, 164 West Xingang Road, Guangzhou 510301, China. wwujun2003@yahoo.com
authors.forename: Jun
authors.initials: J
authors.lastname: Wu
authors.forename: Jianshe
authors.initials: J
authors.lastname: Huang
authors.forename: Qiang
authors.initials: Q
authors.lastname: Xiao
authors.forename: Si
authors.initials: S
authors.lastname: Zhang
authors.forename: Zhihui
authors.initials: Z
authors.lastname: Xiao
authors.forename: Qingxin
authors.initials: Q
authors.lastname: Li
authors.forename: Lijuan
authors.initials: L
authors.lastname: Long
authors.forename: Liangmin
authors.initials: L
authors.lastname: Huang
mesh_terms: D027901:Acanthaceae / Q000378:metabolism*; D002247:Carbon Isotopes; D002681:China; D006027:Glycosides / Q000032:analysis / Q000737:chemistry*; D009682:Magnetic Resonance Spectroscopy / Q000379:methods* / Q000592:standards*; D008958:Models, Molecular; D008968:Molecular Conformation; D010636:Phenols / Q000032:analysis / Q000737:chemistry*; D010936:Plant Extracts / Q000032:analysis / Q000737:chemistry; D011522:Protons; D012015:Reference Standards; D013237:Stereoisomerism
chemical_list: D002247:Carbon Isotopes; D006027:Glycosides; D010636:Phenols; D010936:Plant Extracts; D011522:Protons