Complete assignments of 1H and 13C NMR data for 10 phenylethanoid glycosides.
Ten phenylethanoid glycosides, including two new ones, isolated from the aerial parts of the mangrove plant Acanthus ilicifolius were identified. The first complete assignments of the 1H and 13C NMR chemical shifts for these glycosides were achieved by means of 2D NMR techniques, including 1H-1H COSY, TOCSY, HSQC and HMBC spectra.
Wu
Jun
J
Guangdong Key Laboratory of Marine Materia Medica, South China Sea Institute of Oceanology, Chinese Academy of Sciences, 164 West Xingang Road, Guangzhou 510301, China. wwujun2003@yahoo.com
Huang
Jianshe
J
Xiao
Qiang
Q
Zhang
Si
S
Xiao
Zhihui
Z
Li
Qingxin
Q
Long
Lijuan
L
Huang
Liangmin
L
D027901:Acanthaceae / Q000378:metabolism*; D002247:Carbon Isotopes; D002681:China; D006027:Glycosides / Q000032:analysis / Q000737:chemistry*; D009682:Magnetic Resonance Spectroscopy / Q000379:methods* / Q000592:standards*; D008958:Models, Molecular; D008968:Molecular Conformation; D010636:Phenols / Q000032:analysis / Q000737:chemistry*; D010936:Plant Extracts / Q000032:analysis / Q000737:chemistry; D011522:Protons; D012015:Reference Standards; D013237:Stereoisomerism
D002247:Carbon Isotopes; D006027:Glycosides; D010636:Phenols; D010936:Plant Extracts; D011522:Protons