title: Ochratoxin A in dried vine fruits on the Canadian retail market.
abstract: Between 1998 and 2000, 151 samples of raisins and sultanas and two samples of currants were collected from retail outlets across Canada and analysed for ochratoxin A. Samples were extracted with methanol-sodium bicarbonate, and the extracts were cleaned-up by immunoaffinity column chromatography. Ochratoxin A was quantified by liquid chromatography with fluorescence detection. The minimum quantifiable level was 0.1 ng (g-1). Ochratoxin A was present, above the minimum quantifiable level, in 67 (79%) of 85 samples of raisins, in 39 (59%) of 66 samples of sultanas, and in both samples of currants. The overall mean level of ochratoxin A was 1.8 ng g(-1) in both the raisins and sultanas, and 2.8 ng g(-1) in the currants.
authors.affiliation: Health Canada, Health Products and Food Branch, 510 Lagimodière Blvd, Winnipeg, MB, R2J 3Y1 Canada. gary_Lombeart@hc-sc.gc.ca
authors.forename: G A
authors.initials: GA
authors.lastname: Lombaert
authors.forename: P
authors.initials: P
authors.lastname: Pellaers
authors.forename: G
authors.initials: G
authors.lastname: Neumann
authors.forename: D
authors.initials: D
authors.lastname: Kitchen
authors.forename: V
authors.initials: V
authors.lastname: Huzel
authors.forename: R
authors.initials: R
authors.lastname: Trelka
authors.forename: S
authors.initials: S
authors.lastname: Kotello
authors.forename: P M
authors.initials: PM
authors.lastname: Scott
mesh_terms: D002170:Canada; D002273:Carcinogens / Q000032:analysis; D002851:Chromatography, High Pressure Liquid / Q000379:methods; D005504:Food Analysis / Q000379:methods / Q000592:standards; D005506:Food Contamination / Q000032:analysis*; D006801:Humans; D009793:Ochratoxins / Q000032:analysis*; D027843:Vitis / Q000737:chemistry*
chemical_list: D002273:Carcinogens; D009793:Ochratoxins; C025589:ochratoxin A