Facile characterization of polymer-supported reagents using cross polarization magic angle spinning method in solid state 13C-NMR.
Polymer-supported (PS) reagents can be easily characterized using a cross polarization magic angle spinning method in solid state (13)C-NMR. The technique was applied to the characterization of PS-dimethylimidazolidinone, analogue to potential heterogeneous dehydrating agent.
Shikii
Kazuaki
K
Chemical Analysis Center, Chiba University, Japan.
Seki
Hiroko
H
Yamaguchi
Kentaro
K
Disadee
Wannaporn
W
Watanabe
Toshiko
T
Ishikawa
Tsutomu
T
D002247:Carbon Isotopes; D009682:Magnetic Resonance Spectroscopy / Q000379:methods*; D011108:Polymers / Q000032:analysis* / Q000145:classification*
D002247:Carbon Isotopes; D011108:Polymers