Sample-angle feedback for diffraction anomalous fine-structure spectroscopy.
Diffraction anomalous fine-structure (DAFS) experiments measure Bragg peak intensities as continuous functions of photon energy near a core-level excitation. Measuring the integrated intensity at each energy makes the experiments prohibitively slow; however, in many cases DAFS can be collected quickly by measuring only the peak intensity at the center of the rocking curve. A piezoelectric-actuator-driven stage has been designed and tested as part of a sample-angle feedback circuit for locking onto the maximum of the rocking curve while the energy is scanned. Although software peak-tracking requires only a simple calculation of diffractometer angles, it is found that the additional hardware feedback dramatically improves the reproducibility of the data.
Cross
J O
JO
Naval Research Laboratory, Washington, DC 20375, USA.
Elam
W T
WT
Harris
V G
VG
Kirkland
J P
JP
Bouldin
C E
CE
Sorensen
L B
LB