Crystallization and preliminary X-ray crystallographic analysis of the putative [6Fe-6S] prismane protein from Desulfovibrio vulgaris (Hildenborough).
Crystals of the prismane protein from Desulfovibrio vulgaris (Hildenborough) containing a putative [6Fe-6S] cluster have been obtained and X-ray data collected to a resolution of 1.7 A using synchrotron radiation. The unit cell is orthorhombic with a = 64.1, b = 65.1 and c = 154.1 A, space group P2(1)2(1)2(1) (No. 19). The unit cell will readily accommodate four molecules of molecular weight 60 kDa with a corresponding solvent content of approximately 48%.
Arendsen
A
A
Department of Biochemistry, Agricultural University, Wageningen, The Netherlands.
Bulsink
Y
Y
Hagen
W
W
Hadden
J
J
Card
G
G
McAlpine
A S
AS
Bailey
S
S
Zaitsev
V
V
Lindley
P
P