Quantitative analyses of precession diffraction data for a large cell oxide.
Kinematical and two-beam calculations have been conducted and are compared to experimental precession data for the large unit cell crystal La4Cu3MoO12. Precession electron diffraction intensities are found to exhibit approximate two-beam behavior and demonstrate clear advantages over conventional SADP intensities for use in structure solution.
Department of Materials Science, Northwestern University, 2220 N. Campus Dr., Cook 2036, Evanston, IL 60201, USA. csown@northwestern.edu
Christopher S
CS
Own
Arun K
AK
Subramanian
Laurence D
LD
Marks
D003300:Copper / Q000032:analysis; D003460:Crystallization; D007091:Image Processing, Computer-Assisted; D007811:Lanthanum / Q000032:analysis; D008854:Microscopy, Electron / Q000295:instrumentation / Q000379:methods*; D008982:Molybdenum / Q000032:analysis; D010087:Oxides / Q000737:chemistry*; D014961:X-Ray Diffraction
D010087:Oxides; D007811:Lanthanum; D003300:Copper; D008982:Molybdenum