A review of oxygen-17 solid-state NMR of organic materials--towards biological applications.
17O solid state NMR of organic materials is developing rapidly. This article provides a snapshot of the current state of development of this field. The NMR techniques and enrichment protocols that are driving this progress are outlined. The (17)O parameters derived from solid-state NMR experiments are summarized and the structural sensitivity of the approach to effects such as hydrogen bonding highlighted. The prospects and challenges for (17)O solid-state NMR of biomolecules are discussed.
Lemaître
V
V
Biomembrane Structure Unit, Department of Biochemistry, Oxford University, South Parks Road, Oxford OX1 3QU, UK.
Smith
M E
ME
Watts
A
A
D002625:Chemistry, Organic; D009682:Magnetic Resonance Spectroscopy / Q000379:methods*; D055601:Organic Chemistry Phenomena; D010103:Oxygen Isotopes
D010103:Oxygen Isotopes