Dentin adhesion and microleakage of a resin-based calcium phosphate pulp capping and basing cement.
An experimental resin-based bioactive calcium phosphate cement, intended as a pulp capping and basing material, was evaluated for dentin shear bond strength and microleakage. The interfacial morphology was examined by scanning electron microscopy (SEM). For microleakage, dentin cavities without (Group A) or after (Group B) acid etching were restored with the calcium phosphate cement. A resin-based calcium hydroxide (VLC Dycal; Group C) was used as control material according to the manufacturer's instructions. After water storage and thermocycling, the microleakage was scored using a AgNO(3) staining procedure. For the shear bond strength, flat exposed dentin surfaces were treated as for the microleakage test. Metal irises pressed against the dentin surface were filled with the cements, which were photocured. Both tests were carried out after 1 wk. While acid etching did not result in significantly greater microleakage, it led to higher shear bond strength, and allowed, as shown by SEM, the formation of a hybrid layer and resin tags. Both groups treated with the calcium phosphate cement had significantly lower microleakage scores and higher mean shear bond strength values than the groups treated with the control material.
American Dental Association Foundation, Paffenbarger Research Center, National Institute of Standards and Technology, Gaithersburg, MD 20899, USA. sabine.dickens@nist.gov
Sabine H
SH
Dickens
Sean R
SR
Kelly
Glenn M
GM
Flaim
Anthony A
AA
Giuseppetti
D000134:Acid Etching, Dental; D001565:Benzoates / Q000737:chemistry; D002126:Calcium Hydroxide / Q000737:chemistry; D002130:Calcium Phosphates / Q000737:chemistry*; D001840:Dental Bonding; D003736:Dental Cavity Lining; D003763:Dental Leakage / Q000145:classification*; D003785:Dental Pulp Capping; D003804:Dentin / Q000648:ultrastructure*; D006801:Humans; D008422:Materials Testing; D008689:Methacrylates / Q000737:chemistry; D008855:Microscopy, Electron, Scanning; D008903:Minerals / Q000737:chemistry; D019279:Resin Cements / Q000737:chemistry*; D033081:Shear Strength; D016622:Silver Staining; D013499:Surface Properties
D001565:Benzoates; D002130:Calcium Phosphates; D008689:Methacrylates; D008903:Minerals; D019279:Resin Cements; C080129:pyromellitic dianhydride glycerol dimethacrylate adduct; C074277:ethoxylated bis-phenol A dimethacrylate; C025702:Dycal; C020243:calcium phosphate; D002126:Calcium Hydroxide