Effects of additional and extended acid etching on bonding to caries-affected dentine.
This study evaluated the effects of additional and extended acid etching on microtensile bond strength ( micro TBS) of two adhesive systems to sound (SD) and caries-affected dentine (CAD). Flat surfaces of CAD surrounded by SD of 36 extracted carious third molars were assigned to four treatments (i): self-etching adhesive system (Clearfil SE Bond) applied to dentine surfaces following manufacturer's instructions (MI); (ii) after additional etching for 15 s (35% phosphoric acid, PA); (iii) total-etch one-bottle adhesive (Single Bond) applied to dentine surfaces following MI; or (iv), after etching for 45 s with PA. Composite 'blocks' were built on bonded surfaces and restored teeth were vertically sectioned to obtain bonded slices of 0.7 mm thick. Slices were trimmed to create hourglass-shaped specimens (cross-sectional area of 1 mm(2)), which were tested under tension in a universal testing machine. Additional CAD and SD samples were prepared for scanning electron microscopy observations. Additional and extended etching significantly increased micro TBS to CAD; however, micro TBS of both adhesives to CAD were significantly lower than to SD. Additional and extended etching can improve bonding to CAD; however, adhesives applied on SD showed the best results for bonding.
Department of Restorative Dentistry/Operative Dentistry, Piracicaba School of Dentistry, UNICAMP, Piracicaba, Brazil.
César Augusto Galvão
CA
Arrais
Marcelo
M
Giannini
Masatoshi
M
Nakajima
Junji
J
Tagami
D000134:Acid Etching, Dental / Q000379:methods*; D017438:Bisphenol A-Glycidyl Methacrylate / Q000737:chemistry; D003188:Composite Resins / Q000737:chemistry; D001840:Dental Bonding; D003731:Dental Caries / Q000473:pathology*; D003804:Dentin / Q000648:ultrastructure*; D017220:Dentin-Bonding Agents / Q000737:chemistry*; D006801:Humans; D008422:Materials Testing; D008855:Microscopy, Electron, Scanning; D010756:Phosphoric Acids / Q000737:chemistry; D019279:Resin Cements / Q000737:chemistry; D013499:Surface Properties; D013718:Tensile Strength; D013997:Time Factors
C438313:Clearfil SE Bond; D003188:Composite Resins; D017220:Dentin-Bonding Agents; D010756:Phosphoric Acids; D019279:Resin Cements; C115612:single bond; D017438:Bisphenol A-Glycidyl Methacrylate