Effects of removing residual peroxide and other oxygen radicals on the shear bond strength and failure modes at resin-tooth interface after tooth bleaching.
OBJECTIVE
To investigate the effects of removing residual peroxide on the bond strength and the failure mode at the interface of resin-based composite and enamel after tooth bleaching.


METHODS
Standard-sized light-cured resin cylinders were formed on, and bonded to the flattened bleached enamel surfaces of 60 human canine and premolars which had previously been subjected to three different surface treatments for 3 minutes: (1) catalase; (2) 70% ethanol; (3) sprayed water. For each experimental group (n=12), non-bleached teeth and 2-week post-bleached teeth without any surface treatment were used for negative and positive control respectively. Specimens were thermocycled, tested in shear until failure, and the results statistically analyzed. All fractured specimens were examined by scanning electron microscopy.


RESULTS
Pretreatment of bleached surface with the catalase and the ethanol prior to bonding significantly improved the composite-enamel bond strength compared to the water-sprayed group (P< 0.05). However, the bond strength level of the ethanol group did not return to the level recorded for the non-bleached negative control group. Scanning electron microscopic examination of randomly selected, fractured specimens indicated that the peroxide-induced reduction in bond strength was related to alterations in both attachment-surface area at the resin-enamel interface and resin quality.
Kum
Kee-Yeon
KY
Department of Conservative Dentistry, Oral Science Research Center, College of Dentistry, Yonsei University, Seoul, Korea.
Lim
Kyung-Ran
KR
Lee
Chan-Young
CY
Park
Kwang-Ho
KH
Safavi
Kamran E
KE
Fouad
Ashraf F
AF
Spångberg
Larz S
LS
D000704:Analysis of Variance; D001641:Bicuspid; D002374:Catalase / Q000737:chemistry; D003188:Composite Resins / Q000737:chemistry*; D003481:Cuspid; D001840:Dental Bonding; D000431:Ethanol / Q000737:chemistry; D006801:Humans; D008855:Microscopy, Electron, Scanning; D010545:Peroxides / Q000737:chemistry*; D017382:Reactive Oxygen Species / Q000737:chemistry*; D033081:Shear Strength; D012997:Solvents / Q000737:chemistry; D013499:Surface Properties; D014070:Tooth / Q000648:ultrastructure*; D014073:Tooth Bleaching; D014867:Water / Q000737:chemistry
D003188:Composite Resins; D010545:Peroxides; D017382:Reactive Oxygen Species; D012997:Solvents; D014867:Water; D000431:Ethanol; D002374:Catalase