A succinct method for preparing the Stork-Jung vinylsilane robinson annulation reagent.
The Stork-Jung vinylsilane reagent (1) is prepared in two steps and in good overall yield. This provides rapid and efficient access to a useful methyl vinyl ketone surrogate.
Singletary
Jeananne A
JA
Department of Chemistry and Biochemistry, Florida State University, Tallahassee, Florida 32306-4390, USA.
Lam
Hubert
H
Dudley
Gregory B
GB