title: Deep-penetrating conical cracks in brittle layers from hydraulic cyclic contact.
abstract: A study is made of fracture from cyclic loading of WC spheres on the top surfaces of thick (1 mm) brittle layers on polymeric substrates, as representative of repetitive occlusal contact on dental crown structures. The advantage of glass layers is that internal cracks can be followed in situ during the entire cyclic loading process. The glass surfaces are first given a surface-abrasion treatment to control the flaw state, such that the strengths match those of dental porcelains. Cyclic contact tests are carried out at prescribed maximum loads and frequencies, in water. In addition to conventional cone cracks that form outside the contact circle, additional, inner cone cracks form within the contact in the water environment. These inner cones are observed only in cyclic loading in water and are accelerated at higher frequencies, indicating a strong mechanical driving force. They tend to initiate after the outer cones, but subsequently catch up and penetrate much more rapidly and deeply, ultimately intersecting the underlying coating/substrate interface. Comparative tests on glass/polymer bilayers versus monolithic glass, in cyclic versus static loading, in water versus air environment, on abraded versus etched surfaces, and with glass instead of WC indenters, confirm the existence of a dominant mechanical element in the inner-cone crack evolution. It is suggested that the source of the mechanical driving force is hydraulic pressure from intrusion and entrapment of liquid in surface fissures at the closing contact interface. This new type of cone cracking may limit dental crown veneer lifetimes under occlusal fatigue conditions, especially in thicker layers, where competing modes-such as undersurface radial cracks-are suppressed.
authors.affiliation: Materials Science and Engineering Laboratory, National Institute of Standards and Technology, Gaithersburg, Maryland 20899, USA.
authors.forename: Yu
authors.initials: Y
authors.lastname: Zhang
authors.forename: Jun-Kwang
authors.initials: JK
authors.lastname: Song
authors.forename: Brian R
authors.initials: BR
authors.lastname: Lawn
mesh_terms: D000537:Aluminum Oxide / Q000737:chemistry; D001672:Biocompatible Materials / Q000737:chemistry; D003442:Crowns; D003764:Dental Materials / Q000737:chemistry; D003776:Dental Porcelain / Q000737:chemistry*; D019232:Dental Restoration Failure; D019554:Dental Restoration Wear; D003799:Dental Stress Analysis; D005898:Glass; D008422:Materials Testing; D018715:Microscopy, Video; D011108:Polymers / Q000737:chemistry; D013314:Stress, Mechanical; D013499:Surface Properties; D013718:Tensile Strength; D013997:Time Factors
chemical_list: D001672:Biocompatible Materials; D003764:Dental Materials; D011108:Polymers; D003776:Dental Porcelain; D000537:Aluminum Oxide