Assignment of absolute configuration of 3-hydroxy beta-lactams by the NMR "mix and shake" method.
The absolute configurations of several 3-hydroxy beta-lactams were assigned by the NMR "mix and shake" methodology developed by Riguera and co-workers. The results from the NMR study correlated perfectly with the absolute configurations obtained from X-ray crystallographic structure analyses and chiral-phase HPLC data.
Yang
Yan
Y
Department of Physical Sciences, University of New Brunswick, Saint John, NB, Canada.
Kayser
Margaret M
MM
Hooper
Donald
D
D018360:Crystallography, X-Ray; D009682:Magnetic Resonance Spectroscopy; D008968:Molecular Conformation; D015394:Molecular Structure; D047090:beta-Lactams / Q000737:chemistry*
D047090:beta-Lactams