title: [Analysis of saturated paraffins in petroleum by fast gas chromatography].
abstract: A fast capillary gas chromatographic method for the analysis of saturated paraffin in crude oil and rock extracts is described. By using a 20 m narrow bore capillary column, the analytical time has been shortened to 15 min, 5 times faster in comparison with 80 to 90 min by conventional capillary columns, which resulted in higher throughput, higher efficiency and better separation. The fast method is fully in compliance with the Petroleum Industrial Standard--SY/T5120-1997 and paves the way for the fast analysis of paraffin isomers, such as steroidal paraffin and terpane by gas chromatography/mass spectrometry (GC/MS) and that of aromatics by gas chromatography.
authors.affiliation: Experimental Center, Research Institute of Petroleum Exploration and Development, Beijing 100080, China.
authors.forename: Jie
authors.initials: J
authors.lastname: Wu
authors.forename: Lei
authors.initials: L
authors.lastname: Cao
authors.forename: Yingming
authors.initials: Y
authors.lastname: Li
authors.forename: Yuki
authors.initials: Y
authors.lastname: Hashi
mesh_terms: D002849:Chromatography, Gas / Q000379:methods; D010232:Paraffin / Q000032:analysis*; D010578:Petroleum / Q000032:analysis*; D012680:Sensitivity and Specificity; D013729:Terpenes / Q000032:analysis
chemical_list: D010578:Petroleum; D013729:Terpenes; D010232:Paraffin