Rapid determination of total Kjeldahl nitrogen using microwave digestion.
A closed-vessel microwave digestion process for the determination of total Kjeldahl nitrogen (TKN) has been developed for sewage and wastewater. TKN values obtained from the microwave digestion method were in excellent agreement with those of the thermal digestion method. The accuracy of both analytical methods is comparable. In comparison to the conventional thermal digestion, the microwave method shortened the time required for complete digestion from 4 h to 25 min, and also decreased the maximum digestion temperature from 380 degrees C to 200 degrees C. This developed method may contribute to a significant reduction in sample digestion time, resulting in an increase in analytical throughput. The microwave digestion method developed in this study could be a rapid and efficient means for TKN determination for sewage wastewater and sludge.
Lo
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KV
Department of Civil Engineering, University of British Columbia, Vancouver, British Columbia, Canada. kvlo@interchange.ubc.ca
Wong
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WT
Liao
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PH
D006358:Hot Temperature; D008872:Microwaves; D009584:Nitrogen / Q000032:analysis*; D012722:Sewage / Q000032:analysis; D013997:Time Factors; D014865:Waste Disposal, Fluid; D014874:Water Pollutants, Chemical / Q000032:analysis*
D012722:Sewage; D014874:Water Pollutants, Chemical; D009584:Nitrogen