[Determination of the content of wear metal in lubrication oil by ICP-AES].
An analytical method for determining wear metal elements directly by ICP-AES was proposed in this paper. The optimum condition was selected. The Conostan S-21 and Conostan 75 (oil-base standard samples) prepared by multi-element oil-base reserved standard samples were applied to make calibration curve. Oil samples were diluted 5 times by kerosene. The contents of wear metals in lubrication oil were determined by ICP-AES. The relative standard deviation (RSD) of all elements was less than 1%. In addition, the authors represented the analytical efficacy of Leeman labs multi-track profile ICP, and its rapid and accurate characters of simultaneous multi-element measurement.
Zhao
Jin-wei
JW
Department of Materials Science & Engineering, Nanjing University of Science and Technology, Nanjing 210094, China.
Cheng
Wei
W
Feng
Ya-hui
YH
D002138:Calibration; D004563:Electrochemistry / Q000379:methods; D008153:Lubrication / Q000009:adverse effects; D008670:Metals / Q000032:analysis*; D009821:Oils / Q000737:chemistry*; D010316:Particle Size; D012015:Reference Standards; D013054:Spectrophotometry, Atomic / Q000379:methods*
D008670:Metals; D009821:Oils