1H and 13C NMR data to aid the identification and quantification of residual solvents by NMR spectroscopy.
We present reference data and a javascript web page which allow the rapid identification and quantification of residual solvents by NMR. The data encompass all of the ICH-prescribed solvents and were obtained for a number of NMR solvents. We also present an example of its application.
Jones
Ian C
IC
AstraZeneca, Silk Road Business Park, Macclesfield, Cheshire SK10 2NA, UK. ian.jones@astrazeneca.com
Sharman
Gary J
GJ
Pidgeon
Julia
J
D002247:Carbon Isotopes; D009682:Magnetic Resonance Spectroscopy / Q000379:methods* / Q000592:standards*; D008968:Molecular Conformation; D011522:Protons; D012015:Reference Standards; D012997:Solvents / Q000737:chemistry*
D002247:Carbon Isotopes; D011522:Protons; D012997:Solvents