Synthesis and study on 2,4,6,8-tetraaryl- 3,7-diazabicyclo[3.3.1]nonanes and their derivatives.
1-Carbethoxy-2,4,6,8-tetraaryl-3,7-diazabicyclo[3.3.1] nonan-9-ones (1, 2) were synthesized and their 1H and 13C NMR data are reported. Chemical shifts and spectral assignments for 2,4,6,8-tetrakis(4-chlorophenyl)-3,7-diazabicyclo[3.3.1]nonan-9-one (3), 2,4,6,8-tetraphenyl-3-thia-7-azabicyclo[3.3.1]nonan-9-one (4) and 2,4,6,8-tetraaryl-3,7-diazabicyclo[3.3.1]nonanes (5-7) are also included.
Vijayakumar
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School of Chemical and Biotechnology, Shanmugha Arts, Science, Technology & Research Academy [SASTRA]-Deemed University, Thanjavur-613402, India. kvpsvijayakumar@yahoo.com
Sundaravadivelu
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D000473:Alkanes / Q000138:chemical synthesis / Q000737:chemistry; D019086:Bridged Bicyclo Compounds, Heterocyclic / Q000138:chemical synthesis / Q000737:chemistry; D002247:Carbon Isotopes; D009682:Magnetic Resonance Spectroscopy / Q000379:methods / Q000592:standards; D015394:Molecular Structure; D011522:Protons; D012015:Reference Standards
D000473:Alkanes; D019086:Bridged Bicyclo Compounds, Heterocyclic; D002247:Carbon Isotopes; D011522:Protons; C017573:nonane