HPLC-based procedure for the preparation of carbene-generating photoreactive GM3 and GM1 ganglioside derivatives radioiodinated to high specific radioactivity with chloramine T as an oxidant.
Panasiewicz
Mirosława
M
Department of Biochemistry, Medical Center of Postgraduate Education, 01-813 Warszawa, Poland.
Mieczkowski
Józef
J
Domek
Hanna
H
Pacuszka
Tadeusz
T
D000818:Animals; D002700:Chloramines / Q000737:chemistry*; D002851:Chromatography, High Pressure Liquid / Q000379:methods*; D003978:Diazomethane / Q000031:analogs & derivatives / Q000737:chemistry; D004285:Dogs; D005227:Fatty Acids / Q000737:chemistry; D005233:Fatty Alcohols / Q000737:chemistry; D005677:G(M1) Ganglioside / Q000737:chemistry*; D005679:G(M3) Ganglioside / Q000737:chemistry*; D006838:Hydrocarbons; D007457:Iodine Radioisotopes; D007553:Isotope Labeling / Q000379:methods*; D008697:Methane / Q000031:analogs & derivatives* / Q000737:chemistry; D016877:Oxidants / Q000737:chemistry*; D010777:Photochemistry; D014105:Tosyl Compounds / Q000737:chemistry*; D014220:Trialkyltin Compounds / Q000737:chemistry
C503508:9-(((2-iodo-4-((trifluoromethyl)-3H-diazirin-3-yl)benzyl)oxy)carbonyl)nonanoic acid; C503509:9-(((2-tributylstannyl-4-(trifluoromethyl-3H-diaziryn-3-yl)benzyl)oxy)carbonyl)nonanoic acid; D002700:Chloramines; D005227:Fatty Acids; D005233:Fatty Alcohols; D005679:G(M3) Ganglioside; D006838:Hydrocarbons; D007457:Iodine Radioisotopes; D016877:Oxidants; D014105:Tosyl Compounds; D014220:Trialkyltin Compounds; C016300:chloramine-T; C030011:carbene; D005677:G(M1) Ganglioside; D003978:Diazomethane; D008697:Methane