[Determination of 15 trace rare earth elements in rice by microwave digestion ICP-MS].
An ICP-MS method for direct determination of 15 trace rare earth elements in rice was developed. Rapid and complete dissolution of rice was achieved by a microwave digestion procedure with concentrated nitric acid and hydrogen peroxide. The detection limits are 7.0-25.8 pg/mL, the recoveries for spiked samples are 95-105%, RSDs are 2.3-4.2%. This method is rapid, sensitive and accurate.
Liu
M
M
Public Health College, Beijing Medical University, 100083 Beijing.
Liu
H
H
Wang
N
N
Wang
X
X
D057230:Limit of Detection; D013058:Mass Spectrometry; D008674:Metals, Rare Earth / Q000032:analysis* / Q000737:chemistry*; D008872:Microwaves; D012275:Oryza / Q000737:chemistry*; D015203:Reproducibility of Results
D008674:Metals, Rare Earth