Optimization of isotope-labeling conditions for lambertellin based on isotope patterns observed by mass spectrometry.
A method for the sensitive analysis of the incorporation level of labeled acetate was developed. This method allowed for the optimization of the conditions for lambertellin with up to 48% average incorporation of labeled acetate.
Murakami
Takanori
T
Faculty of Agriculture and Life Science, Hirosaki University, 3-Bunkyo-cho, Hirosaki 036-8561, Japan.
Sasaki
Akane
A
Fukushi
Eri
E
Kawabata
Jun
J
Hashimoto
Masaru
M
Okuno
Toshikatsu
T
D007553:Isotope Labeling; D009682:Magnetic Resonance Spectroscopy; D013058:Mass Spectrometry / Q000379:methods*; D009281:Naphthalenes / Q000737:chemistry*; D013141:Spiro Compounds / Q000737:chemistry*
D009281:Naphthalenes; D013141:Spiro Compounds; C504281:lambertellin