title: EBSD FEG-SEM, TEM and XRD techniques applied to grain study of a commercially pure 1200 aluminum subjected to equal-channel angular-pressing.
abstract: Microstructural evolution due to equal-channel angular-pressing (ECAP) with increasingly severe deformation was investigated in a commercially pure 1200 aluminum alloy. A true strain of eight produced sub-micrometer scale grains and very fine subgrains in the grain interior. The deformation process was documented and described using field-emission (FEG) gun scanning and transmission electron microscopy techniques. After eight ECAP passes, the high-angle grain boundaries accounted for approximately 70% of all boundaries. The fine spacing resolution of FEG scanning electron microscopy allowed detailed grain and subgrain statistical evaluation in the deformed microstructure; transmission electron microscopic inspection afforded appreciation of the role of very low-angle misorientation boundaries in the microstructure-refining process. ECAP results were compared with those produced by cold rolling. The material's texture evolved in a decreasing trend of Cube {001}100 intensities in favor of Cube rotated toward the normal-to-pressing direction {001}120, while Goss {110}001 and {111}110, {111}112 directions slightly increased with strain.
authors.affiliation: INFM/Dipartimento di Meccanica, Università Politecnica delle Marche, Via Brecce Bianche, 60131 Ancona, Italy. marcello.cabibbo@univpm.it
authors.forename: M
authors.initials: M
authors.lastname: Cabibbo
authors.forename: E
authors.initials: E
authors.lastname: Evangelista
authors.forename: C
authors.initials: C
authors.lastname: Scalabroni