title: Seven-year dentin bond strengths of a total- and self-etch system.
abstract: The aim of this study was to determine the durability of tensile bond strengths of a conventional 3-step bonding system (Superbond D-liner Plus) and a self-etching priming bonding system (Clearfil Liner Bond II) to bovine dentin over a 7 yr period. Superficial bovine dentin finished with 600-grit SiC paper was bonded with one of the two adhesive materials. A 4 mm diameter area was bonded, covered with resin composite and stored in 37 degrees C deionized water containing gypsum chips and 0.4% sodium azide as an antibacterial. Bonds were stressed in tension at a crosshead speed of 1 mm min(-1). Mean bond strengths were observed at 1 d, at 1, 3, and 6 months, and at 1, 2, 3, 6 and 7 yr. Ten specimens were tested for the first 3 yr and 15 specimens were tested for 6 and 7 yr. The bond strength of Superbond D-liner Plus significantly decreased over the 7 yr period, whereas Liner Bond II showed a slight but, insignificant, decrease. The fracture mode changed with time for Superbond D-liner Plus, but not for Liner Bond II. It was concluded that systems which use a strong acid for demineralizing the dentin may show greater deterioration of the bond to dentin compared with a self-etching priming system.
authors.affiliation: School of Dental Science, The University of Melbourne, Parkville, Victoria 3010, Australia. mfburrow@unimelb.edu.au
authors.forename: Michael F
authors.initials: MF
authors.lastname: Burrow
authors.forename: Naoko
authors.initials: N
authors.lastname: Harada
authors.forename: Yuichi
authors.initials: Y
authors.lastname: Kitasako
authors.forename: Toru
authors.initials: T
authors.lastname: Nikaido
authors.forename: Junji
authors.initials: J
authors.lastname: Tagami
mesh_terms: D000134:Acid Etching, Dental / Q000379:methods; D000818:Animals; D002417:Cattle; D003188:Composite Resins / Q000737:chemistry; D001840:Dental Bonding; D003804:Dentin / Q000648:ultrastructure; D017220:Dentin-Bonding Agents / Q000737:chemistry*; D008422:Materials Testing; D008689:Methacrylates / Q000737:chemistry; D019279:Resin Cements / Q000737:chemistry; D013314:Stress, Mechanical; D013499:Surface Properties; D013696:Temperature; D013718:Tensile Strength; D013997:Time Factors; D014867:Water / Q000737:chemistry
chemical_list: C112274:Clearfil Liner Bond 2; D003188:Composite Resins; D017220:Dentin-Bonding Agents; D008689:Methacrylates; D019279:Resin Cements; C084543:Super Bond D-Liner; D014867:Water