Rapid pulse length determination in high-resolution NMR.
The 90 degrees (1H) pulse length can be determined in a single scan using a simple homo-gated decoupling/nutation experiment. We show that the method is fast, accurate and readily amenable to automation.
Wu
Peter S C
PS
Research School of Chemistry, Australian National University, Canberra, ACT 0200, Australia.
Otting
Gottfried
G
D000818:Animals; D002645:Chickens; D009113:Muramidase / Q000737:chemistry*; D019906:Nuclear Magnetic Resonance, Biomolecular / Q000379:methods*
D009113:Muramidase