[Synthesis and character of megastigmatrienone].
In this synthetic route, the raw materials are obtained easily and the conditions of reactions are smoothly. The products in some main procedures of the route have high yieds. This synthetic route is a new way of the compound, there hasn't been reported anywhere. It needs further studies to be practically applied. According to this synthetic routes, the authors studied technolygical conditions of the reactions of every step. Some products are analyzed by refractive index, IR, HNMR, and MS and confirmed its structure.
Wang
Jian-lin
JL
Material and Chemical Engineering College of Zhengzhou University of Light Industry, Zhengzhou 450002, China.
Yang
Shao-long
SL
Xu
Yan-mei
YM
Zhao
Qing-hua
QH
Qian
Lan
L
D001688:Biological Products / Q000138:chemical synthesis / Q000737:chemistry*; D003512:Cyclohexanones / Q000138:chemical synthesis / Q000737:chemistry*; D009682:Magnetic Resonance Spectroscopy; D013058:Mass Spectrometry; D015394:Molecular Structure; D009930:Organic Chemicals / Q000138:chemical synthesis / Q000737:chemistry*; D012031:Refractometry; D013055:Spectrophotometry, Infrared; D013237:Stereoisomerism
D001688:Biological Products; D003512:Cyclohexanones; D009930:Organic Chemicals; C549856:(4Z)-4-((E)-but-2-enylidene)-3,5,5-trimethylcyclohex- 2-en-1-one