A novel miniaturized flame ionization detector for portable gas chromatography.
A novel miniaturized flame ionization detector (FID) operated by battery, which can be used as a detector in portable gas chromatography (GC) is devised and manufactured. It is characterized by the structure of building blocks, small volume, low energy consumption, and needing only two gases, which can be used for detection of hydrocarbons in portable GC. The miniaturized detector mainly includes a porous metallic diffuser plate, bugle-figuration collector, quartz capillary flame tip, and self-heated system. The miniaturized FID is easy to fabricate and assemble because of its structure of building blocks. The FID response is linear over six orders of magnitude and the detection limit of 0.518 ng for benzene, 0.430 ng for n-dodecane, 0.473 ng for naphthalene, and 0.509 ng for n-tetradecane.
Deng
Chunhui
C
Department of Chemistry, Fudan University, Shanghai 200433, China.
Yang
Xiuhan
X
Li
Ning
N
Huang
Yue
Y
Zhang
Xiangmin
X
D000473:Alkanes / Q000032:analysis; D001554:Benzene / Q000032:analysis; D002849:Chromatography, Gas / Q000295:instrumentation*; D005410:Flame Ionization / Q000295:instrumentation*; D008904:Miniaturization / Q000379:methods; D009281:Naphthalenes / Q000032:analysis; D015203:Reproducibility of Results
D000473:Alkanes; D009281:Naphthalenes; C024713:n-tetradecane; C007548:n-dodecane; C031721:naphthalene; D001554:Benzene