[Microwave-assisted route to fibre-like ternary NaFeS2 nanoparticles and its XPS].
Ternary NaFeS2 nanoparticles were obtained in aqueous solution at room temperature via microwave-assisted route. The products were fibre-like with the diameter less than 10 nm, which were characterized with X-ray diffraction (XRD) pattern, transmission electron microscope (TEM) image, selected area electron diffraction (SAED) pattern and X-ray photoelectron spectroscope (XPS) pattern. The results indicated that the composition of fibre-like ternary nanoparticles are with atomic ratio of Na:Fe:S=1:1.1:1.9. The mechanism for the formation of fibre-like NaFeS2 nanoparticles is discussed.
Wu
Hua-qiang
HQ
College of Chemistry and Materials Science, Anhui Normal University, Wuhu 241000, China.
Shao
Ming-wang
MW
Gu
Jia-shan
JS
Wei
Xian-wen
XW
D005290:Ferric Compounds / Q000737:chemistry*; D046529:Microscopy, Electron, Transmission; D008872:Microwaves; D053758:Nanoparticles / Q000737:chemistry* / Q000648:ultrastructure; D056951:Photoelectron Spectroscopy / Q000379:methods*; D013440:Sulfides / Q000737:chemistry*; D014961:X-Ray Diffraction
D005290:Ferric Compounds; D013440:Sulfides; C518794:sodium ferric sulfide