Determination of aflatoxins in peanuts, maize feed and whole milk by HPLC-MS2 and MS3 tandem mass spectrometry.
A method is presented for the detection of six toxins of fungal origin in various foods: peanuts, a sample of maize feed and whole milk. Extraction and HPLC-APCI-MS detection were discussed. The performances of MS/MS, MS3 and SRM detection modes were checked and best conditions of sensitivity were obtained in MS/MS mode.
Pazzi
Marco
M
Dipartimento di Chimica Analitica, Università di Torino, Via P. Giuria 5, 10125 Torino, Italy. marco.pazzi@unito.it
Medana
Claudio
C
Brussino
Mariacarla
M
Baiocchi
Claudio
C
D000348:Aflatoxins / Q000032:analysis*; D000818:Animals; D010367:Arachis / Q000737:chemistry*; D002851:Chromatography, High Pressure Liquid; D013058:Mass Spectrometry / Q000379:methods; D008892:Milk / Q000737:chemistry*; D003313:Zea mays / Q000737:chemistry*
D000348:Aflatoxins