A novel fiber coating for solid phase microextraction and its application for the extraction of n-alkane from aqueous sample.
Base on the previous work in laboratory, a novel polyaniline doped with polydimethylsiloxane coating was developed on a stainless steel wire for solid phase microextraction(SPME) by electroplating method. This electroplating method not only has advantages of ease preparation and simple equipments required, but also increases the lifetime of the SPME fiber. The composite fiber (polyaniline/ polydimethylsiloxane(PANI/PDMS)) was evaluated by analyzing n-tridecane, n-tetradecane and n-pentadecane in aqueous sample. The new fiber coating showed comprehensive abilities to extract alkanes compounds. The relative standard deviations were found to be 6.8%-10.33%.
Huang
Min-jia
MJ
State Key Laboratory of Environmental Chemistry and Ecotoxicology, Research Center for Eco-Environmental Science, Chinese Academy of Sciences, Beijing 100085, China.
Jiang
Gui-bin
GB
Zhao
Zong-shan
ZS
Liu
Ji-yan
JY
D000473:Alkanes / Q000032:analysis*; D000814:Aniline Compounds / Q000737:chemistry*; D002849:Chromatography, Gas; D004129:Dimethylpolysiloxanes / Q000737:chemistry*; D004595:Electroplating / Q000379:methods*; D008855:Microscopy, Electron, Scanning; D012828:Silicones / Q000737:chemistry*; D014874:Water Pollutants, Chemical / Q000032:analysis*; D018508:Water Purification / Q000295:instrumentation* / Q000379:methods
D000473:Alkanes; D000814:Aniline Compounds; D004129:Dimethylpolysiloxanes; D012828:Silicones; D014874:Water Pollutants, Chemical; C416807:polyaniline; C013830:baysilon