Simple protocol for NMR analysis of the enantiomeric purity of primary amines.
[reaction: see text] A practically simple three-component chiral derivatizing protocol for determining the enantiopurity of 13 chiral primary amines by (1)H NMR spectroscopic analysis is described, including analysis of those that contain remote stereocenters.
Department of Chemistry, University of Bath, Bath, BA2 7AY, UK.
Yolanda
Y
Pérez-Fuertes
Andrew M
AM
Kelly
Andrew L
AL
Johnson
Susumu
S
Arimori
Steven D
SD
Bull
Tony D
TD
James
D000588:Amines / Q000032:analysis* / Q000737:chemistry*; D009682:Magnetic Resonance Spectroscopy / Q000379:methods*; D015394:Molecular Structure; D013237:Stereoisomerism
D000588:Amines