[Isolation and structure identification of the chemical constituents from Gypsophila oldhamiana].
OBJECTIVE
To study the constituents of the root of Gypsophila oldhamiana Miq.


METHODS
Silica gel column chromatographic technique was used for the isolation and purification of compounds. The structures were elucidated on the basis of spectral data and chemical evidences.


RESULTS
Five compounds were obtained and identified as the beta-D-glucoside of alpha-spinasterol (I), tetracosyl caffeate (II), sucrose (III), beta-sitosterol (IV) and daucosterol (V).


CONCLUSIONS
Compound II is a new compound. Compound I was isolated from this plant for the first time.
Sun
Jing-yong
JY
Institute of Materia Medica. Shandong Academy of Medical Sciences, Jinan 250062, China.
Zhong
Ying
Y
Zuo
Chun-xu
CX
Yin
Jun-ting
JT
Wang
Bin
B
D002109:Caffeic Acids / Q000737:chemistry / Q000302:isolation & purification*; D029748:Caryophyllaceae / Q000737:chemistry*; D008968:Molecular Conformation; D015394:Molecular Structure; D018517:Plant Roots / Q000737:chemistry; D010946:Plants, Medicinal / Q000737:chemistry*; D013265:Stigmasterol / Q000031:analogs & derivatives* / Q000737:chemistry / Q000302:isolation & purification; D013395:Sucrose / Q000737:chemistry / Q000302:isolation & purification
D002109:Caffeic Acids; C031312:spinasterol; D013395:Sucrose; D013265:Stigmasterol