Simple protocol for NMR analysis of the enantiomeric purity of primary amines.
[reaction: see text] A practically simple three-component chiral derivatizing protocol for determining the enantiopurity of 13 chiral primary amines by (1)H NMR spectroscopic analysis is described, including analysis of those that contain remote stereocenters.
Pérez-Fuertes
Yolanda
Y
Department of Chemistry, University of Bath, Bath, BA2 7AY, UK.
Kelly
Andrew M
AM
Johnson
Andrew L
AL
Arimori
Susumu
S
Bull
Steven D
SD
James
Tony D
TD
D000588:Amines / Q000032:analysis* / Q000737:chemistry*; D009682:Magnetic Resonance Spectroscopy / Q000379:methods*; D015394:Molecular Structure; D013237:Stereoisomerism
D000588:Amines