Liquid chromatography with accurate mass measurement on a triple quadrupole mass-spectrometer for the identification and quantification of N-lactoyl ethanolamine in wine.
In this study a specific taste-modulating flavor ingredient, N-lactoyl ethanolamine, was determined in two Beerenauslese wines using preparative LC, as a first isolation and concentration step, followed by LC-MS/MS on a triple quadrupole in accurate mass (AM) mode. The accurate masses of the analyte and three characteristic fragments were determined with mass accuracies between 8 and 20 ppm. N-lactoyl ethanolamine concentrations in the wines were 0.4 and 2.5 mg/L.
de Rijke
Eva
E
Quest International, Department of Analytical Research and Development, GP Naarden, The Netherlands.
Ruisch
Bart J
BJ
Bouter
Nico
N
König
Thorsten
T
D005591:Chemical Fractionation; D002853:Chromatography, Liquid / Q000379:methods*; D004983:Ethanolamines / Q000032:analysis*; D019344:Lactic Acid / Q000031:analogs & derivatives* / Q000032:analysis; D013058:Mass Spectrometry / Q000379:methods*; D021241:Spectrometry, Mass, Electrospray Ionization; D014920:Wine / Q000032:analysis*
D004983:Ethanolamines; D019344:Lactic Acid; C510961:N-lactoylethanolamine