[Chemical constituents from root of Lasianthus acuminatissimus I].
OBJECTIVE
To investigate the chemical constituents from the root of Lasianthus acuminatissimus of Rubiaceae.


METHODS
Normal, reverse phase silica gel, macroporous resin column and HPLC chromatography were used for isolation. Spectroscopic methods (13C-NMR, 1H-NMR, DEPT, EI-MS) were used for identification.


RESULTS
Six compounds were isolated and elucidated as isoscopletin(I), isoscopletin-6-O-beta-D-glucopyranoside (II), beta configuration of Mudanoside-A (Ill), asperuloside (IV), (-)-pinoresinol 4-O-beta-D-glucopyranoside (V), daucosterol (VI).


CONCLUSIONS
These compounds were obtained from this plant for the first time.
Li
Bin
B
Jiangxi University of Traditional Chinese Medicine, Nanchang 330006, China.
Zhang
Dong-Ming
DM
Luo
Yong-Ming
YM
D000081004:Cyclopentane Monoterpenes; D005960:Glucosides / Q000737:chemistry / Q000302:isolation & purification*; D006027:Glycosides / Q000737:chemistry / Q000302:isolation & purification*; D017705:Lignans / Q000737:chemistry / Q000302:isolation & purification*; D018517:Plant Roots / Q000737:chemistry; D010946:Plants, Medicinal / Q000737:chemistry*; D011714:Pyrans / Q000737:chemistry / Q000302:isolation & purification*; D019666:Rubiaceae / Q000737:chemistry*; D012855:Sitosterols / Q000737:chemistry / Q000302:isolation & purification
D000081004:Cyclopentane Monoterpenes; D005960:Glucosides; D006027:Glycosides; D017705:Lignans; D011714:Pyrans; D012855:Sitosterols; C530440:pinoresinol 4-O-glucopyranoside; C111731:mudanoside B; C011015:lyoniside; C077956:asperuloside